By G. W. C. Milner, G. M. Phillips and R. J. Magee (Auth.)
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Extra info for Coulometry in Analytical Chemistry
UO2* + 2H+ + 2e = U4+ + H2. At a stirred-mercury electrode the copper reduction is reversible in dilute sulphuric acid solutions, whereas the uranium is not. On applying a potential of — 0-325 V vs. E. to the mercury electrode, both copper and uranium are reduced in accordance with the above equations and the copper forms an amalgam with the mercury. 15 CONSTANT-POTENTIAL COULOMETRY 27 Fe2+/Fe3+ Log [Ox] [Red] -2 0-8 07 0-6 05 0-4 V vs. E. Working electrode potential FIG. 10, Plot of coulogram for iron and plutonium in HCl solution.
C. motor at this voltage. However, deviations from linearity greater than 0-5% could be produced by using input voltages less than 5 V. This characteristic is very inconvenient as it limits any flexibility in applying this system. However, some of these difficulties have been overcome in an apparatus developed by Smythe10 in which the use of two integrating motors enables a wide range of currents to be available and allows end points to be approached slowly. The circuit for this instrument is shown in Fig.
Nat. 3. DEFORD, Bur. St. 6 3 A , 2 ( 1 9 5 9 ) . D . D . , J O H N S , C . J. a n d P I T T S , J. N . , Analyt. (1951). 4. REILLEY, C. N . , COOKE, W . D . a n d F U R M A N , N . H . , Analyt. (1951). 5. REILLEY, C. N . , A D A M S , R. N . and F U R M A N , 8. B E T T , N . , N O C K , W . a n d M O R R I S , G . , Analyst Chem. 2 3 , 1 0 3 0 N . H . , Analyt. 1044(1952). 6. F U R M A N , N . H . , SAYEGH, L. J. and A D A M S , R . N . , Analyt. (1955). 7. WHEATLEY, B . M . , British J.
Coulometry in Analytical Chemistry by G. W. C. Milner, G. M. Phillips and R. J. Magee (Auth.)